CHEMISTRY TODATY

WELCOME TO CHEMISTRY WORLD

Friday, February 18, 2011

prepare nano materials

LETTER FROM RK SIVAKUMAR TO ME :
 good afternoon ,this method is very easy and cheaf.we prepare nano materials by using

deionised water.we can prepare ag,zr,co,cr,al,zn nano material by this method.

  • 3 mg of metal powder was (like Ag ions) added to 30 ml deionized water in a glass veil
  • the reaction mixture was sonicated for about 15 min in a glass,transfered in to a stainless steel teflon linked metallic
         bomb of 100 ml capacity and sealed under normal condition

the closed chamber was then placed inside the a preheated box furnace and the mixture was heated slowly
2 c/min to 200 c and maintained the temp for 612 hours.
  • the furnace is allowed to cool after the desired time and the suspension was centrifuged to retrive the product,washed 
        and finally dried using vaccum air for few hours .the powder can be analise by using SEM

mechasim:
                    Agno3+nabh 4 ? Ag +no2+water

No comments:

Post a Comment